My first batch that doesnt have amonia smell uses these oil too. Read more about sodium lactate here: http://www.soapqueen.com/bramble-berry-news/sunday-night-spotlight-sodium-lactate/, You can also water discount your soap! Then add amount desired to melted soap base. The titanium dioxide lightens the soap and makes them a lot prettier. You may be able to use it as laundry detergent though! . The result is the appearance of moisture, tears, sweating or dew drops on the melt and pour. 2%jojoba. I have only made about five small batches and each one has been its own learning event. Reason: Zinc oxide or titanium dioxide wasn't completely blended into the soap batter, leaving little white flecks in the soap. The absolute may be separating because its not meant for use in balms. Finally ready to make my lard soap, hopefully! When I poured the lye into the oils I poured it through a sifter just to make sure there was no undissolved lye present. Any ideas about what happened? I'll keep experimenting! This is because its particles have a relatively high refractive index. I am going to check the pH of 2 different batches of soap immediately using the cabbage method AND pH strips, but no separation has been apparent. If you prefer a harder bar, I would recommend increasing the hard oils. Oh no, Im sorry to hear that! Read more about sodium lactate here: http://www.soapqueen.com/bramble-berry-news/sunday-night-spotlight-sodium-lactate/, Hi, With the 8% oil missing, the soap may be lye heavy. As for how much titanium dioxide is needed in soap, it depends a bit on your batter! I used 5% lye and they both crumbled when I cut them. Learn more about working with honey here: https://www.soapqueen.com/bath-and-body-tutorials/tips-and-tricks/adding-honey-to-cold-process-soap-tips-tricks-recipe/. or so into my batch and I have perfect white soap. When I add my lye to the water it usually begins at around 200 degrees and then drops somewhat to the mid hundreds then takes a little longer to get below 100. What can I do in order for the bottom is the soap to be as hard and set as the top? Feel free to share, tweet and pin to your hearts content. How long are you stick blending for, and how are you storing the soap? You can post now and register later. Thanks! It has been ground into a fine powder, and delivers maximum whiteness and opacity when added to products. Placed the soap there for 7 hours, removed from freezer and left it in room temperature (approx 28 degrees C) for 12 hours, then attempted to cut. [3] It is also resistant to ultraviolet (UV) light, and is . If the pH is safe to use, the crumbly texture could also be caused by soaping with cool temperatures. How to Fix it:To avoid ricing and seizing, make sure your fragrance oils have been tested for cold process soap (good news, all Bramble Berry Fragrance Oils are thoroughly tested in soap!) You can read more about burnt melt and pour here: https://www.soapqueen.com/bath-and-body-tutorials/tips-and-tricks/how-to-avoid-burnt-melt-pour/, To prevent the soap from burning, we recommend heating it on very short bursts as short as 5 seconds. , See how to rebatch soap in this recipe: http://www.soapqueen.com/bath-and-body-tutorials/cold-process-soap/soap-queen-tv-presents-how-to-make-rebatch-soap-2/, You can use the Fragrance Calculator to find out how much to use in your recipe: https://www.brambleberry.com/Pages/Fragrance-Calculator.aspx. Titanium Dioxide (TD) is a pigment used in soap making to turn soap into the color white. I asked on a facebook group and they said because my recipe used a lot of soft oils, the oil might reabsorb in time. Let me know and Ill help you troubleshoot. I would recommend testing a small amount on your clothing to see what you think. Soap with DOS my also develop an unpleasant odor. Soap that contains too much colorant is safe to use on the body, but could potentially stain wash cloths. I have a whole pound of this stuff and im wasting fragrance oils and oils . I just made a few soaps and when I unmolded them they were oily. My recipe is the lots of lather. What can I do to make them feel more moisturizing? My bars are still nice without orange spots. That one was sticky too. Is there a quicker way to dry these bars? It should be around 9-10 pH. Some people have concerns about its use because there has been a lot of buzz lately about possible carcinogenic effects of titanium dioxide. Hmm, the lumps could be several things! Turn off the heat and Google for creative options to deal with a soap mess-up. added oatmeal in one and honey on the other. , Liquid glycerin: https://www.brambleberry.com/Glycerin-Liquid-P5965.aspx. TiO2 occurs in many silicates in nature, accounting for over 1% of the earth's crust. Constituent Profice:44.7% Linalyl Acetate, 28% linalook, 8.1% coumarin, 1.2% Camphor, 0% Limonene, 0% Geraniol, 0% 1,8-Cineol. That involves grating the soap and heating it on the stove. I wonder if those bars are separating. EVOO 8% (50g) I am experimenting with gel phase lately. Using Titanium Dioxide in Your Soap. If I use soaps, makeup, mascara, with it, my eyes go CRAZY, and the first syptoms are large under eye bags and swelling and drying. . The thing about TD depends on your recipe because each combo of oils is different in everyone's recipe. I used the lye about a week ago on another bar of soap with no problem. Hmm, Im not quite sure why that happened! Or the texture could feel chalky or powdery. If you pinpoint the problem, let us know. To prevent that, we like to micronize it. Some soapers swear by it and use it to prolong essential oils??? /r/soapmaking is a place to share your soap making tips and tricks, links to cool techniques, ask soaping related questions or just fun new soap designs you've found or created. Titanium dioxide is safely used in many products from paint and food to drugs and cosmetics. Sadly, it was so crumbly that it kept breaking apart while cutting. Hot Process Hero It doesnt affect the final bar, but it can form ash on the top and make it crumbly. Ive been wondering if its something to do with colorants because some seem to behave worse than others. Titanium dioxide is actually one of the most widely used colorants in the world. The first is that titanium dioxide can help to adsorb impurities from the soap solution. You can use more but please be aware the more you use will increase the chance it may migrate into other colors. This gives an intense white colour. Titanium is a common metal element mined from the earth and is also found in animals and plants. What would happen if I added too much? Revised IDLH: 5,000 mg/m 3 Basis for revised IDLH: The available toxicological data contain no evidence that an acute exposure to a high concentration of titanium dioxide would impede escape or cause any irreversible health effects within 30 minutes. Thank you! Pure Fine Titanium Dioxide (TiO2) Food-Grade Safe Colorant | Pigment, Toothpaste, Edible Use | Vegan Friendly, Non-GMO | Resealable Bag (PTR-213) 16oz/8oz/4oz (8oz/0.5lb) 8 Ounce (Pack of 1) 4.6 out of 5 stars 309 $14.98$14.98 ($14.98/Ounce) FREE delivery Fri, Nov 4 on $25 of items shipped by Amazon Or fastest delivery Tue, Nov 1 Small Business 2% rosehip. Are the bars developing orange discoloration or an unpleasant smell? That is especially the case with recipes with more soft oils. Titanium Dioxide Common Name Ingredient Listing (FDA Approved): Titanium Dioxide Directions: MP Soap: Add color to a small amount of liquid glycerin. These spots can appear in one area of the soap, or all over. I am so sorry for the long wait! But does not give a perfect white. What essential oil are you using, and what oils in your recipe? If its dangerous or caustic at all, you may need to toss the coconut oil. It was very strange that during blending, it never got to trace. For a better experience, please enable JavaScript in your browser before proceeding. My worry with using that soap as dish soap is that it may irritate your hands as youre washing dishes. I can take a pic once I'm home again just for confirmation. I put mine directly into my oils and stick blend it in with my oils and lye solution. How green is your olive oil? You can find it in products ranging from paint and plastics to food and cosmetics. Thanks so much for that recipe! Click here to learn about how to turn your lye-heavy soap into usable laundry soap. I microwaved it again but that just made it form a thick skin on top. Pure titanium dioxide has an anatase content of 80% by weight with a smaller portion of rutile, 20%. The soap has cured between 1-3 weeks so far. The soap on the right does not contain sodium lactate, while the soap on the left does. Also, are the bumps white? Titanium dioxide power is very fine-grained and it agglomerates, so glazes containing it need to be sieved to break down the small lumps (even a high-speed propeller mixer often won't do it). These are also an aberrant form of glycerin "rivers". Goat Milk Stuff LLC76 S Lake Road NScottsburg, IN 47170, http://www.cdc.gov/niosh/docs/2011-160/pdfs/2011-160.pdf, http://www.ncbi.nlm.nih.gov/pubmed/4002222, http://www.ccohs.ca/headlines/text186.html, http://www.organicmakeup.ca/ca/titaniumdioxide.asp. Reddit and its partners use cookies and similar technologies to provide you with a better experience. Id love to see a picture to confirm though. Just to confirm, you waited about 24 hours before cutting the soap? Can i use it this way? Within 30 minutes it was at GEL phase all the way through and had turned a dark cardboard brown. Below is the recipe percentage: Pure Olive 32% (230g) If you tell me a bit more about your recipe Id be happy to help you troubleshoot! Can be used singly or in a blend. I typically soap around 120 degrees. This is not at all what the report states, implies, or construes. It looks like dried T.D, but Im not sure how to prevent this. Titanium dioxide is also an occupational chemical of concern, as workers might inhale titanium dioxide when manufacturing products. DOS (Dreaded Orange Spots) Its chemical structure makes it ideal for refracting light and its particle size allows it to disperse evenly throughout a formulation, which is why it is ideal for whitening or creating opacity in food and beverage applications. Hi guys, I'm having trouble getting my soap white! i love the water dispensable from nurture myself. That's very fast to develop DOS - are you sure it's DOS? 2 tbsp ground oatmeal. Can you tell me a bit more about your recipe, and how hot youre soaping? Many of these fixes include rebatching the soap, which involves melting the soap with a small amount of additional liquid. Do you notice any odd smell from the oils themselves? If the balm doesnt separate, it is likely the absolute causing the trouble. It certainly was not hard to slice. Or, are they the same color as your soap? Hi Kelsey, I am curing it for 4-6 weeks So I am not sure why these bars came out like this. every time i add the lye it ether immediately gets so thick I cant use the stick blender or it take FOREVER to trace and instead of tracing it separates theres always this weird grainy stuff on the top and melted oils underneath after what seems like eternity its will start to thicken up but its like mashed potatoes except is smooth and instead of cooling down is heating up with out me doing anything to it except stirring! I guess its normal for some soaps to dry longer in between uses depending on the recipe. Im curious now! Titanium dioxide has been problematic for rats forced to inhale large quantities, or who have had it injected directly into their trachea (thus bypassing the nasal filtering mechanisms). How to Fix it: Unfortunately there is no way to get rid of air bubbles once the soap has been made, other than rebatching or using the hot process hero technique. My soap has been getting hard bubbles that look like tiny beads all over it. In fact, I love this soap, its so creamy and soft on my hands. I used castor oil 5%, coconut 30%, olive oil 35%, palm 30%, lye 4 oz, milk 9.24. I did the test it did not turn brown, but I cant figure out what it is and if the soaps would be safe to sell. It also helps to adjust your microwave settings to low so it heats gently. It is also commonly used in sunscreens and countless other applications including coloring products white. Ill include some recipes below. Your link has been automatically embedded. When I used them for the first time they left my skin a bit dry. Works great to give you a clean white bar of soap, and mixes really easily in the CP soap - no streaking or clumping. I hardly point out what problem i am facing now. You guys are really amazing. Luckily, there methods to prevent and fix these blunders. We add a tiny amount because those three soaps tend to take on a grey hue. I thought maybe somehow condensation of moisture developed when I was heating it up and the moisture was at the bottom of it .I see only when I look at the underside of the dish.I then decided to crack it up to break up the balm in chunks to see more.Then I saw white covering it too.Is it MOLD? If youre finding the soap is 11 pH or higher, it could be your scale. Want to receive discounts and special offers and stay up to date with all the latest news? That makes it gloppy, or form a skin, or harden really quickly. Not recommended for lotion or bath bombs. Instead of the typical off white soap color, the Titanium Dioxide will create a more pure white color in your bars. http://www.ccohs.ca/headlines/text186.htmlThis, however, will not be a problem for anyone who has it in the soap they are using in the shower. If you notice your soap is really hot, you can leave it at room temperature uncovered, or even pop it in the fridge or freezer to keep it cool. The European Union just published the official delegated regulation to classify titanium dioxide as a suspected carcinogen by inhalation. It is moisturizing that is for sure! Also, the soap may just need a bit longer in the freezer next time! Ricing occurs when an ingredient in the fragrance oil binds with some of the harder oil components in the recipe to form little hard rice-shaped lumps (shown on the left). The good news is its purely aesthetic and doesnt affect the final bars. The third one recipe is your beautiful swirl but i used sweet almond instead of hazelnut oil. I have just made some goats milk melt and pour soaps with English rose fragrance oil, and I used 1 drop of red food colouring (I use it all the time as colourant) I also put a rose bud on top. It is cosmetically safe for general use, lips . I don't know what gives. Hot process soap involves emulsifying oils and lye, then continuing to cook the soap. I have researched on how to re-batch but Im not sure whats wrong with my soap. of TD and stir. I did make the mistake of adding a bit of fragrance (only 20 drops for a 50 oz batch) after reaching a medium trace (last time I wasnt sure I reached trace, so I overcompensated this time). It can also be the palm oil or butters in your recipe. How could I save them? What does PPO stand for? 24 hours later, the top is covered in a good amount of oil and the center appears to still be soft. Thank you very much for the info, Sponiebr!! Soap containing air bubbles will have small lumps or bumps within the soap, as shown below. This will give you a nice pearlescent effect. The soap was definitely lye heavy. I ended up using the soaps in the shower for myself because they have plenty of time to dry in between uses. I did stir time to time to help everything melt especially the bee wax pellets. The second benefit of titanium dioxide is that it's non-toxic and relatively safe to use. It requires precise measuring of properly selected ingredients to initiate the saponification process. To prevent soda ash, increase the temperature of your lye and oils to 120F-140F. We use 99% isopropyl alcohol all the time in the Soap Lab. I rarely use TD, so can't be sure on that one. I figured I used too much even though I followed directions perfectly. Several factors can cause crumbly soap, including sodium lactate. , Also, Amanda with Lovin Soap has an awesome blog post that talks about how to neutralize liquid soap using citric acid. Soap made with only soft oils can take an extremely long time to unmold (such as castile soap). Didnt feel like water. You can find that post here: http://www.lovinsoap.com/2010/09/liquid-soap-neutralizing-and-superfating/, Thanks Kelsey, it is all learning! So with this i have cooked it longer and the translucent stage came about after about 3 1/2 hours with some liquid deposits which i was sure if it was water or what. Burnt melt and pour hardens up very quickly and forms a skin on top. If melt and pour soap gets too hot, it can burn. Oatmeal soap came out just fine. Then, add the dispersed colorant 1 teaspoon at a time until you get a nice white color. . What else I could with this soap? Unrefined Shea Butter 10% (70g) DOS looks exactly like it soundsorange or rust colored spots on your soap. So I only used about 1.5 teaspoons. Enter your email address below and you will receive all our new posts directly in your email inbox. What are your suggestions moving forward? When doing so, be aware that further stick blending may result in an extremely thick trace. If the soap has stayed in the mold for 2+ weeks and is still extremely soft, it will most likely not harden. If youre making a larger batch, you may need to mix 2 teaspoons of the colorant into 2 tablespoons of oil, or 3 teaspoons into 3 tablespoons. Using a draining soap dish can help as well. Titanium Dioxide Common Name Ingredient Listing (FDA Approved): Titanium Dioxide Directions: MP Soap: Add color to a small amount of liquid glycerin. Become a part of the GMS family when you sign up for our newsletter. You cannot paste images directly. Typically, sodium lactate shouldnt cause that batch to seize. Additives were colloidal oatmeal and bentonite clay. Hello, I just made my second batch of soap ever (formulated my own recipe with 60% hard oils etc) with coconut oil, olive oil, palm oil, cocoa butter, unrefined shea butter and castor oil. Unlike all of the other lavenders, Lavender Absolute is not steam distilled. I soaped with Greek olive oil once and it was super yellow. I pour the soup in the mold and put it in the oven for an even warming. Soda ash occurs on soap due to the natural process of unsaponified lye reacting with carbon dioxide in the air. Im determined to make this soap again. Another oddity that can happen from the heating of TD laden soap is something called glycerin rivers. I test the ph and it is good. Glycerin rivers are all throughout this soap, which was made with titanium dioxide and high temperatures. Is it possible to hot process soap after the fact if the scent didnt turn out the way you wanted? Use the plastic or ceramic bowl to weigh your lye. Yep, common things that go wrong and how to fix [], 2022 Soap Queen Site Design by Emily White Designs. Plus, the TRUTH about vanilla stabilizers from suppliers & learn how to make your own vanilla stabilizer for only $0.05 an ounce! The River Runs Deep: An Explanation of Glycerin Rivers I would recommend pH testing the soap. If you are worried about your soap being lye heavy, check out this blog post to test the pH using strips, cabbage or even your tongue. DOS doesn't typically occur untilafter weeks of curing, not days, unless the oils used were rancid to begin with, but you would have smelled that while soaping. I would recommend waiting 5 days and then pH testing the soap. When it comes out of the fridge, it can start to sweat. You can definitely use that for laundry soap if you like! Thanks so much for the advice!. The titanium dioxide lightens the soap and makes them a lot prettier. PPO for most batches. At this point the soap can be used as is although it will not last very long and the lather may be lacking. But dont throw your lye-heavy soap away! Can you tell me a bit more about your recipe, including the colorants youre using? I'm just say'n, BE aware of this. I followed the instructions on the titanium dioxide which was .5 teaspoons per pound of oils. , Learn how to pH test the bars and how to make laundry soap here: https://www.soapqueen.com/bath-and-body-tutorials/tips-and-tricks/troubleshooting-lye-heavy-soap/. The top is exposed to air right away, giving it time to harden. Display as a link instead, It also helps to water discount that soap by 10% or so. Im sorry about that Charity! It turned very thick, as thick as thick trace in cold process. You can find it easily without titanium dioxide, just look for transparent m&p. Sorbitan oleate will be in all of it because (like I said) without it the soap wouldn't be meltable or pourable. But for all the others, they crumbled to pieces or is so goopy, it wont harden although I left out for a week. Will let it set for a few days. That can definitely happen with titanium dioxide! It is now day 3 since the soap was made and while the top of the soap is hard and set, when trying to unfold I am seeing where at the bottom it sticking to the mold. I figured I used too much even though I followed directions perfectly. Answer (1 of 3): Titanium dioxide but may cause glycerine rivers if used in excess. Plus, an overload of powdered TiO . 10%Shea. I use the oil dispersable one but it also dissolves quite nicely in water too. When a portion of palm oil is melted, it may not contain all the necessary fatty acids that your soap requires. Its really helpful. You may want to try a skin-safe essential oil intended for balms. Im sorry about that! Soda ash normally occurs on the top of the soap. Oh no, Im sorry about that! I cut through it and while the outside was fine the inside had gone through a gel phase and it was crumbly, but not hard. Any help would be wonderful. Glycerin rivers are more likely to occur in soap containing oxides, particularly Titanium Dioxide. 2.5 tsp per pound of oils (or 2 tsp per pound of soap) in CP Soap. Once the soap has seized, there is no way to return it to a fluid texture. I use a pint jar. Thanks! I could see one batch being heavy but all my batches. ETA: I should have added it sounds more like FO spots, than DOS.. When inserting the stick blender into the oils, burp the stick blender by tapping the blender on the bottom of your container. It helps to sprinkle a very small amount and then blow to evenly distribute the product. It may be something else causing that smell! Let me know and well get this figured out. I have left out oils in my batch before as well. We often use lye heavy cold process soap as laundry soap, so liquid soap should be similar. If the soap does not contain enough lye, the oils will not saponify. or so into my batch and I have perfect white soap. Tried to make something that would look like crystals Press J to jump to the feed. However, it cleans and suds well with a strong clean smell. , Read more about common soapmaking oils and how much to use in this post: http://www.soapqueen.com/bath-and-body-tutorials/tips-and-tricks/free-beginners-guide-to-soapmaking-common-soapmaking-oils/. Some soap can take weeks to unmold depending on a variety of factors so you may just have to wait it out too. The new regulation on titanium dioxide will apply in September 2021. It is a white, water-insoluble solid, although mineral forms can appear black. They can actually look pretty cool in my opinion, but generally they are considered a "flop" by soapmakers TD can also make tiny, titchy, pinpoints of transparent dots when dispersed throughout the batter in high water content soap. Great. So breathe easy; the few varieties of Goat Milk Stuff soap that contain tiny amounts of titanium dioxide (black raspberry,clean cotton, andocean)will not cause cancer when used properly. I am not sure I agree with the above. Oh darn, Im sorry about that! When glycerine is used in soap, clusters of glycerine can be found. Read more about how to water discount here: http://www.soapqueen.com/bath-and-body-tutorials/tips-and-tricks/water-discounting-cold-process-soap-how-why/. I was making a 2lb batch of soap and and tried to use sodium lactate to harden bars of soap. Better base colour as. As an oxide, titanium is found in minerals in the earth's crust. It soaps beautifully! and 2) if I do rebatch, should I add more essential oil to the soap? I think the fragrances likely caused the color. I premixed the clay with the essential oils and it seemed well incorporated when I added it at trace. I use Kaolin clay, it's natural, hardens the bar, helps to fix the fragrance in the soap. As so often happens, headline writers took some liberty in summarizing the report leading many people to believe that the titanium dioxide that they see as an ingredient in their bath & body products, cosmetics, toiletries and even food could be putting them at risk for cancer. It seems i was about 20 grams too high on the KOH over 450grams of Virgin Coconut. Hmmm. coconut, palm, and olive oil should give you a nice white bar. Also, you will be able to still use your personal cold process soaping recipe. How long does it usually take for coconut oil to trace? This rich, verdant oil is FOR PERFUME USE ONLY. For stearic acid, a naturally vegetable-derived waxy substance, .5 ounce per pound of oils is sufficient to produce a hard soap. (just found out it means "pounds per oil" but that didn't make sense when I heard someone say "I use X amount after PPO". But Im not satisfy with the final output Im facing so much of a problem of soap hardening As soon as Im removing my soap flakes from a microwave, it immediately gets hardened So 1/3rd portion of my soap gets wasted What shall I do for it??
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